IGCSE Chemistry 0620 Paper 63, May/June 2026

Question paper and mark scheme40 marks4 questions

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Question paper

0620/63 · May/June 2026

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1

A student uses the apparatus in Figure 1.1 to investigate the electrolysis of sodium chloride.

Figure 1 of 1 for question 1
a

Name the item of apparatus labelled A in Figure 1.1.

[1]
b

State the general term used for the positive electrode, B, in Figure 1.1.

[1]
c

Give one observation, other than effervescence, during the electrolysis in Figure 1.1.

[1]
d

Suggest one change to the apparatus so the student can collect the gas made at electrode B in Figure 1.1.

[1]
e

Describe how the student can confirm that chlorine is made at electrode B in Figure 1.1.

[2]
f

Suggest one safety precaution the student must take when carrying out the experiment shown in Figure 1.1.

[1]
2

A student investigates the temperature change when sodium thiosulfate is dissolved in water. The student does five experiments. Experiment 1 • Place a polystyrene cup into a 250 cm3 beaker for support. • Use a 25 cm3 measuring cylinder to pour 20 cm3 of distilled water into the polystyrene cup. • Use a thermometer to measure the initial temperature of the distilled water. • Add 1.0 g of sodium thiosulfate powder to the distilled water in the polystyrene cup and immediately start a stop-watch. Stir the mixture with the thermometer. • Measure the temperature of the solution at 1 minute. • Rinse out the polystyrene cup with distilled water. Experiment 2 • Repeat Experiment 1 using 2.0 g of sodium thiosulfate powder instead of 1.0 g. Experiment 3 • Repeat Experiment 1 using 3.0 g of sodium thiosulfate powder instead of 1.0 g. Experiment 4 • Repeat Experiment 1 using 4.0 g of sodium thiosulfate powder instead of 1.0 g. Experiment 5 • Repeat Experiment 1 using 5.0 g of sodium thiosulfate powder instead of 1.0 g.

Figure 1 of 1 for question 2
a

Use the information in the description of the experiments and the thermometer diagrams to complete Table 2.1. Calculate the temperature change using the equation shown. temperature change=initial temperature−final temperature Table 2.1

[5]
b

On Figure 2.1, write a suitable scale on the y-axis and plot your results from Experiments 1 to 5. Draw a line of best fit.

[4]
c

On Figure 2.1, extrapolate your line of best fit to deduce the temperature change if 5.7 g of sodium thiosulfate powder is added to 20 cm3 of distilled water. Show clearly on Figure 2.1 how you worked out your answer. temperature change = .........................................°C

[3]
d

Suggest why sodium thiosulfate powder is used in the experiments rather than large lumps.

[1]
e

Explain why it would be an improvement to measure the volume of distilled water in a burette rather than a measuring cylinder.

[1]
f

State if the energy change when sodium thiosulfate powder is dissolved in distilled water is exothermic or endothermic. Use the results in Table 2.1 to explain your answer. energy change .......................................................................................................................... explanation ................................................................................................................................

[1]
g

Suggest why it is an improvement to use a lid on the polystyrene cup.

[1]
h

Suggest why the initial temperature of the distilled water does not need to be the same in each experiment.

[1]
i

The energy change in a reaction is calculated using the equation shown. energy change=volume of water×4.18×temperature change Calculate the energy change when sodium thiosulfate powder dissolves in Experiment 3. energy change = ....................................................... J

[1]
3

A student tests two substances: solution A and solid B. Tests on solution A Table 3.1 shows the tests and the student’s observations for solution A. Table 3.1

a

State what conclusion can be made about solution A from the observations in test 1.

[1]
b

State what conclusion can be made about solution A from the observations in test 2.

[1]
c

A flame test is used to confirm the identity of the cation in solution A. Describe how to carry out a flame test.

[2]
d

Suggest what the sodium carbonate reacts with in test 4 to produce carbon dioxide gas.

[1]
e

Tests on solid B Solid B is zinc sulfate. The student dissolves solid B in water to form solution B. The student divides solution B into three approximately equal portions into one boiling tube and two test-tubes. Complete the expected observations. To the first portion of solution B in the boiling tube, the student adds aqueous sodium hydroxide dropwise and then in excess. observations ..............................................................................................................................

[2]
f

To the second portion of solution B in a test-tube, the student adds 1 cm3 of dilute nitric acid followed by a few drops of aqueous barium nitrate. observations ........................................................................................................................

[1]
g

To the third portion of solution B in a test-tube, the student adds 1 cm3 of dilute nitric acid followed by a few drops of aqueous silver nitrate. observations ........................................................................................................................

[1]
4

Rhubarb plant leaves contain oxalic acid. Oxalic acid is soluble in water. Acidified aqueous potassium manganate(VII) changes from purple to colourless when it reacts with oxalic acid. Plan an experiment to find which of two rhubarb plant leaves, A and B, contains the highest concentration of oxalic acid. You are provided with two rhubarb plant leaves, A and B, acidified aqueous potassium manganate(VII) and common laboratory apparatus.

[6]

Mark scheme

0620/63 · May/June 2026

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1a · 1 mark

  • 1 mark

    beaker

1b · 1 mark

  • 1 mark

    anode

1c · 1 mark

  • 1 mark

    lamp lights up

1d · 1 mark

  • 1 mark

    place a test-tube over the anode

1e · 2 marks

  • M1

    (damp) litmus

  • M2

    bleaches / turns white

1f · 1 mark

  • 1 mark

    use a fume cupboard

2a · 5 marks

  • M1

    all masses of sodium thiosulfate correct

  • M2

    initial temperatures correct

  • M3

    final temperatures correct

  • M4

    all temperature changes correct

  • M5

    all values shown to 1 dp

2b · 4 marks

  • M1

    y-axis scale in linear and points extend over halfway up scale above zero

  • M2

    All points plotted correctly (part 1)

  • M3

    All points plotted correctly (part 2)

  • M4

    ruler drawn line of best-fit ignoring the anomaly at point 4 and passes through the origin

2c · 3 marks

  • M1

    extrapolation to 5.7 g on the graph

  • M2

    a vertical line from 5.7 g to the extrapolation AND a horizontal line back to the y-axis

  • M3

    correct value

2d · 1 mark

  • 1 mark

    to increase the rate of dissolving

2e · 1 mark

  • 1 mark

    (more) accurate

2f · 1 mark

  • 1 mark

    endothermic and temp decreases / gets cooler

2g · 1 mark

  • 1 mark

    so energy is not taken in from the surroundings

2h · 1 mark

  • 1 mark

    measuring a temp change

2i · 1 mark

  • 1 mark

    20  4.18  5 = 418

3a · 1 mark

  • 1 mark

    calcium ions

3b · 1 mark

  • 1 mark

    chloride ions

3c · 2 marks

  • M1

    description of using a non-luminous / blue / roaring (Bunsen) flame

  • M2

    description of how the substance is put into the flame – on a wire / on a splint / spray a solution

3d · 1 mark

  • 1 mark

    sulfuric acid

3e · 2 marks

  • M1

    white precipitate

  • M2

    soluble (in excess)

3f · 1 mark

  • 1 mark

    white precipitate

3g · 1 mark

  • 1 mark

    remains colourless / no change

4 · 6 marks

  • 1 mark

    known / stated / same mass of leaves

  • 1 mark

    grind / crush with water

  • 1 mark

    known / set volume of leaf solution / (oxalic) acid or manganate (aliquote)

  • 1 mark

    use of flask / beaker appropriate for manganate(VII) / acid reaction

  • 1 mark

    add one reagent to other until colour changes

  • 1 mark

    mix / swirl during addition

  • 1 mark

    correct conclusion statement

Questions

  1. 1
    Question 17 marks
    Mark scheme ›
  2. 2
    Question 218 marks
    Mark scheme ›
  3. 3
    Question 39 marks
    Mark scheme ›
  4. 4
    Question 46 marks
    Mark scheme ›

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